Vapor Phase Application of JPX and JPX-E
Preparatory:
Obtain simplified process flow
diagram review; with operations, the sequence and priority for equipment
decontamination. Mark up diagram to show
JPX injection points and vent locations; show flow path for vapor cleaning
through process vessels.
Prepare a layout page showing
sequence and volumes of JPX (or JPX-E).
Time, temperature, results, and rinse columns will be completed as
application proceeds.
Application:
Prior to pumping JPX, verify the following, by physically checking:
1) Vessel is drained – Condensate not hydrocarbon coming from bottom drain
connection. Do not rely on control
instrument levels. They may be plugged
or blocked in.
2) Vessel is vented to relief system, sometimes called blowdown or vapor
recovery system.
3) JPX injection valves into vessel are open, and that only one flow path
for JPX exists.
4) Check and record vessel temperature.
Depending on system flow and vessel size, temperature should be over
200°F after a couple of hours of steaming.
5) Check rinse line (reflux line) to be free of H.C. and hot via steam.
Begin pumping JPX
into vessel:
Typically one drum per 20 minutes.
After pumping ½ of the calculated JPX required, re-check drain line, any
top vent connection and reflux (rinse) line for JPX lemon odor to verify
vaporization is adequate. When
completed, JPX injection continue steaming for several more hours; then have
operations lower steam rates dropping vessel pressure and perform sniff for
LEL, benzene, and H2S. If
vessel is a column, the overhead accumulator would have JPX injected
immediately after column JPX injection and would be sniffed at the same time as
column.
If sniff OK, start fresh water rinse, hot water is preferred. Maximize flow of rinse & continue for
several hours until bottom drain is clear of soap emulsion. Caution, do not use accumulator water or
reflux pump as water rinse source.
Accumulator may have sludge emulsion from JPX cleaning and could
recontaminate column.
After:
Complete layout
page info and discuss with operations.
Flush JPX pumps with water.
Remove empty JPX drums to location for later pick up.